Mild hydrothermal preparation of a layered metal hydroxide salt with microtube/rod morphology--颗粒学报PARTICUOLOGY

Zhang, H., Li, H., Guo, Y., Li, G., Fan, C., Wang, K., & Chen, J. (2010). Mild hydrothermal preparation of a layered metal hydroxide salt with microtube/rod morphology. Particuology, 8(3), 192-197. https://doi.org/10.1016/j.partic.2010.03.009

Mild hydrothermal preparation of a layered metal hydroxide salt with microtube/rod morphology

He Zhang ^{a b}, Hongbin Li ^a, Ying Guo ^b, Guodong Li ^b, Chi Fan ^b, Keji Wang ^b, Jiesheng Chen ^a *

a School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, China
b State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry, Jilin University, Changchun 130012, China

10.1016/j.partic.2010.03.009

Volume 8, Issue 3, June 2010, Pages 192-197

Received 10 January 2009, Accepted 19 May 2009, Available online 2 April 2010.

E-mail: chemcj@sjtu.edu.cn

Highlights

Abstract

Microtubes/rods of the layered metal hydroxide salt compound Cd₂(OH)₃(DS)·nH₂O, where DS stands for dodecyl sulfate sandwiched between two adjacent inorganic sheets, have been synthesized for the first time through a mild hydrothermal reaction route. The microtubes/rods have a diameter of about 1 μm and a length ranging from several microns to 20 μm. The growth process of microtubes/rods under the experimental conditions employed follows a dissolution–recrystallization route.

Graphical abstract

Keywords

Layered metal hydroxide salt; Cadmium hydroxide; Microtubes/rods; Hydrothermal reaction; Dodecyl sulfate; Micelle

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