Additive free microwave assisted synthesis of nanocrystalline Mg(OH)2 and MgO--颗粒学报PARTICUOLOGY

Bhatte, K. D., Sawant, D. N., Deshmukh, K. M., & Bhanage, B. M. (2012). Additive free microwave assisted synthesis of nanocrystalline Mg(OH)2 and MgO. Particuology, 10(3), 384–387. https://doi.org/10.1016/j.partic.2011.05.004

Additive free microwave assisted synthesis of nanocrystalline Mg(OH)2 and MgO

Kushal D. Bhatte, Dinesh N. Sawant, Krishna M. Deshmukh, Bhalchandra M. Bhanage^*

Department of Chemistry, Institute of Chemical Technology, N. Parekh Marg, Matunga, Mumbai 400019, India

10.1016/j.partic.2011.05.004

Volume 10, Issue 3, https://www.sciencedirect.com/science/article/pii/S1674200111001696#aep-abstract-id16, Pages 384-387

Received 14 March 2011, Revised 4 May 2011, Accepted 13 May 2011, Available online 9 November 2011.

E-mail: bm.bhanage@ictmumbai.edu.in; bm.bhanage@gmail.com

Highlights

Abstract

A novel approach for additive free synthesis of nanocrystalline magnesium hydroxide (MH) and magnesium oxide (MgO) using microwave technique is herein reported. Use of 13-propanediol as a solvent played multiple roles circumventing the additional requirement of any extraneous species such as base and other capping agents. The prepared nanomaterials were well characterised using TEM, XRD, EDAX, Raman spectroscopy and FT-IR analysis.

Graphical abstract

Keywords

Nanostructures; Microwave; Mg(OH)₂; MgO; 1,3-Propanediol

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