Coating of finely dispersed particles by two-fluid nozzle--颗粒学报PARTICUOLOGY

Hampel, N., Roydeva, E., Bück, A., & Tsotsas, E. (2018). Coating of finely dispersed particles by two-fluid nozzle. Particuology, 38, 80-93. https://doi.org/10.1016/j.partic.2017.05.015

Coating of finely dispersed particles by two-fluid nozzle

N. Hampel ^*, E. Roydeva, A. Bück, E. Tsotsas

Thermal Process Engineering, Otto von Guericke University, Universitätsplatz 2, 39106 Magdeburg, Germany

10.1016/j.partic.2017.05.015

Volume 38, June 2018, Pages 80-93

Received 29 September 2016, Revised 25 April 2017, Accepted 10 May 2017, Available online 20 October 2017, Version of Record 2 April 2018.

E-mail: neli.ivanova@ovgu.de

Highlights

• New approach for coating fine dispersed particles (d < 50 μm).

• Comparison between the measured and calculated suspension viscosity.

• Calculated liquid film thickness to be used to predict the formation of agglomerates.

• Influence of significant (process) parameters on product quality of coated particles.

Abstract

Particle coatings are used extensively to generate dispersed solids with well-defined properties, e.g., to protect active ingredients, with most coating processes using core particles of a diameter larger than 200 μm. This work contributes to the development of a coating process for fine dispersed particles (diameter less than 50 μm) by combining two particle-formulation processes, namely, coating and spray drying. The feasibility of the operation is based on and demonstrated by the innovative application of a two-fluid nozzle. Experiments were conducted by using glass particles as core particles and sodium benzoate as the coating agent. The coating of finely dispersed particles is achieved by the spraying of particles and coating solution as a homogeneous suspension. The aim is to create droplets with only one contained particle at the nozzle outlet. After evaporation of the water in the droplet, a thin solid film is built on the particle surface. The suspension viscosity was measured and compared with empirical equations from the literature. The liquid-film thickness on the particle surface was calculated to predict the building of a uniform coating layer or agglomerates. In this study, the feasibility of pneumatic transport through the nozzle and an investigation of the process were illustrated. The agglomeration fraction and degree of coating of the particle surface were analyzed optically by scanning electron microscopy. In this way, the influence of different processes and suspension parameters on the product quality were determined.

Graphical abstract

Keywords

Coating; Spray drying; Fine dispersed particle; Two-fluid nozzle

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