Volume 106
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Oil shale separation performance and apparent viscosity characteristics in a ternary dense medium high-density gas–solid fluidized bed
Pengfei Zhao a b c, Guangjian Ren a b c, Chuanxin Fang e, Zongsheng Sun a b c, Fan Yang a b c, Guangqing Zhu a c d, Chenyang Zhou a b c, Bo Zhang a b c *
a Key Laboratory of Coal Processing and Efficient Utilization of Ministry of Education, China University of Mining & Technology, Xuzhou, 221116, China b School of Chemical Engineering & Technology, China University of Mining & Technology, Xuzhou, 221116, China c Jiangsu Key Laboratory for Clean Utilization of Carbon Resources, China University of Mining & Technology, Xuzhou, 221116, China d School of Low Carbon Energy and Power Engineering, China University of Mining and Technology, Xuzhou, 221116, China e CCTEG Wuhan Engineering Company, China
10.1016/j.partic.2025.08.022
Volume 106, November 2025, Pages 70-80
Received 7 August 2025, Revised 25 August 2025, Accepted 27 August 2025, Available online 5 September 2025, Version of Record 11 September 2025.
E-mail: bzhang@cumt.edu.cn; zhangbocumt@126.com

Highlights

• Effect of medium gradation on bed viscosity was investigated.

• Viscosity distribution in fluidized bed was clarified.

• Viscosity impact on particle settling behavior was revealed.

• Optimal viscosity range for efficient separation was defined.


Abstract

Efficient dry separation is essential for utilizing low-grade oil shale. This study developed a ternary high-density gas–solid fluidized bed system using ferrosilicon powder, magnetite powder, and D-class oil shale particles, focusing on the impact of apparent viscosity on particle settling. Results showed that viscosity was influenced by medium composition, particle size, and flow structure. In the binary system of B− silicon and B+ magnetite, minimum viscosity (0.782 Pa s) was reached at a 40 % ferrosilicon ratio. In the ternary system, viscosity increased nonlinearly with oil shale content, with 8 % being the critical threshold where fluidization stability declined. Gas velocity significantly affected viscosity distribution, with moderate increases improving flow uniformity and reducing viscosity by 32 %–40 %. However, excessive velocity caused bubble coalescence and increased viscosity fluctuations, with standard deviation rising from 0.0065 to 0.0191 Pa s. Sedimentation tests showed that the middle bed region provided optimal separation at low gas velocity, while higher velocities shifted separation to the upper region. When gas velocity exceeds 0.45 m/s, the best separation efficiency is achieved. This study clarifies the relationship between viscosity and separation performance, providing guidance for optimizing dry oil shale separation.

Graphical abstract
Keywords
Gas–solid fluidized bed; Ternary dense medium; Apparent viscosity; Oil shale separation; Particle settling dynamics